Our group has developed and successfully used an in-situ measurement setup for the study hydrothermal formation of nanoparticles under sub- and supercritical conditions. The presentation introduces details of the experimental setup as well as explaining each step of the data analysis. As an example of one of our experiment some preliminary results of a temperature and concentration study for hydrothermal synthesis of spinel type LiMn2O4, which is a well-known cathode material for Lithium ion batteries, will be presented.
In-situ synchrotron powder X-ray diffraction
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